BH GSO ISO 6721-10:2016
ISO 6721-10:1999
Bahraini Standard
Current Edition
·
Approved on
08 February 2016
Plastics -- Determination of dynamic mechanical properties -- Part 10: Complex shear viscosity using a parallel-plate oscillatory rheometer
BH GSO ISO 6721-10:2016 Files
English
15 Pages
Current Edition
Reference Language
BHD
30.34
BH GSO ISO 6721-10:2016 Scope
This part of ISO 6721 specifies the general principles of a method for determining the dynamic rheological
properties of polymer melts at angular frequencies typically in the range 0,01 rad.s1 to 100 rad.s1 by means of an
oscillatory rheometer with a parallel-plate geometry. Angular frequencies outside this range can also be used (see
note 1). The method is used to determine values of the following dynamic rheological properties: complex shear
viscosity *, dynamic shear viscosity ', the out-of-phase component of the complex shear viscosity '', complex
shear modulus G*, shear loss modulus G'' and shear storage modulus G'. It is suitable for measuring complex shear
viscosity values typically up to approximately 10 MPa.s (see note 2).
NOTE 1 The angular-frequency measurement range is limited by the specification of the measuring instrument and also by
the response of the specimen. When testing using angular frequencies lower than 0,1 rad.s–1 the test time can increase
significantly as the time taken to obtain a single measurement is proportional to the reciprocal of the angular frequency.
Consequently, when testing at low angular frequencies degradation or polymerization of the specimen is more likely to occur
and have an effect on the results. At high angular frequencies the specimen may distort or fracture at the edge, consequently
invalidating the test results.
NOTE 2 The range of complex shear viscosity values that can be measured is dependent on the specimen dimensions and
also the specification of the measuring instrument. For a specimen of given dimensions, the upper limit of the range is limited
by the machine's torque capacity, angular-displacement resolution and compliance. However, correction can be made for
compliance effects.
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